Chapter 11: Catalysis

B.Sc. 2nd Year Chemistry – Detailed and Exam-Oriented Notes

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1. Introduction

Catalysis is the phenomenon in which the rate of a chemical reaction is altered by the presence of a substance called a catalyst, which is not consumed overall in the reaction.

A catalyst generally increases the rate of a reaction by providing an alternative reaction pathway with a lower activation energy. In some cases, substances called negative catalysts or inhibitors decrease the rate of reaction.

Important: A catalyst changes the rate at which equilibrium is reached but does not change the equilibrium constant or the final equilibrium composition of a reversible reaction.

Catalysis is extremely important in industrial chemistry, petroleum processing, environmental chemistry, biological systems and the manufacture of important chemicals.

2. Catalyst

A catalyst is a substance that changes the rate of a chemical reaction without undergoing permanent overall chemical change at the end of the reaction.

The catalyst may participate in individual elementary steps and may form intermediate compounds, but it is regenerated during the overall catalytic cycle.

Example

The decomposition of hydrogen peroxide is slow in the absence of a suitable catalyst but is greatly accelerated by substances such as manganese dioxide.

2H2O2 → 2H2O + O2

MnO2 acts as a catalyst and is not consumed in the overall reaction.

3. Characteristics of Catalysts

4. Positive and Negative Catalysis

4.1 Positive Catalysis

When a substance increases the rate of a chemical reaction, the phenomenon is called positive catalysis.

Example: Manganese dioxide accelerates the decomposition of hydrogen peroxide.

2H2O2 MnO₂ 2H2O + O2

4.2 Negative Catalysis

When a substance decreases the rate of a reaction, the phenomenon is called negative catalysis.

Such substances are often called inhibitors or retarders.

In biological and industrial systems, inhibitors may be deliberately used to slow undesirable reactions such as oxidation or decomposition.

5. Homogeneous Catalysis

In homogeneous catalysis, the catalyst and reactants are present in the same physical phase.

For example, in a liquid-phase reaction, both the reactants and catalyst may be present in the same solution.

Example: Oxidation of Sulfur Dioxide

Nitric oxide can participate in the oxidation of sulfur dioxide through a homogeneous gas-phase catalytic mechanism.

2SO2 + O2 → 2SO3

Nitric oxide participates in intermediate steps and is regenerated.

6. Heterogeneous Catalysis

In heterogeneous catalysis, the catalyst and reactants are present in different physical phases.

A common example is a solid catalyst used in a gas-phase reaction.

Example: Haber Process

N2 + 3H2 ⇌ 2NH3

Finely divided iron is used as the catalyst in the industrial manufacture of ammonia.

Example: Hydrogenation of Vegetable Oils

Unsaturated oil + H2 Ni More saturated product

Nickel provides an active surface on which hydrogen and the organic molecules can adsorb and react.

7. Homogeneous and Heterogeneous Catalysis

Homogeneous catalysis Heterogeneous catalysis
Catalyst and reactants are in the same phase. Catalyst and reactants are in different phases.
Reaction occurs throughout the phase. Reaction commonly occurs at the catalyst surface.
Separation of catalyst may be difficult. Solid catalysts can often be separated easily.
Mechanisms may involve soluble intermediates. Adsorption and surface reactions are often important.

8. Autocatalysis

Autocatalysis occurs when one of the products formed during a reaction acts as a catalyst for the same reaction.

Example

In the oxidation of oxalate ions by permanganate ions in acidic medium, Mn2+, one of the products, accelerates the reaction.

2MnO4 + 5C2O42− + 16H+ → 2Mn2+ + 10CO2 + 8H2O

The reaction initially proceeds slowly and becomes faster as Mn2+ accumulates.

9. Induced Catalysis

Induced catalysis refers to a situation in which one reaction influences or facilitates another reaction that would otherwise occur very slowly under the same conditions.

The phenomenon can occur when a species generated in one reaction participates in or promotes another reaction.

Induced catalysis is different from autocatalysis because the accelerating species is not necessarily a product of the reaction being accelerated.

10. Enzyme Catalysis

Enzymes are biological catalysts produced by living organisms. Most enzymes are proteins, although some catalytic RNA molecules also exist.

Enzymes accelerate biochemical reactions under mild conditions and generally show high specificity toward their substrates.

Example

The enzyme catalase accelerates the decomposition of hydrogen peroxide.

2H2O2 catalase 2H2O + O2

Important Characteristics of Enzyme Catalysis

11. Enzyme-Substrate Complex

Enzyme catalysis is commonly explained by the formation of an enzyme-substrate complex.

E + S ⇌ ES → E + P

Where:

The substrate binds to a specific region of the enzyme known as the active site.

12. Lock-and-Key Model

The lock-and-key model, proposed by Emil Fischer, describes the enzyme active site as having a shape complementary to the substrate.

According to this model, the substrate fits into the active site in a manner similar to a key fitting into a lock.

The lock-and-key model helps explain enzyme specificity, although the modern induced-fit model provides a more flexible description of enzyme-substrate binding.

13. Induced-Fit Model

The induced-fit model, associated with Daniel Koshland, proposes that the enzyme active site can undergo a conformational change when the substrate approaches.

Binding of the substrate induces a suitable structural arrangement that facilitates the reaction.

This model explains both enzyme specificity and the ability of enzymes to stabilize the transition state.

14. Catalysis and Activation Energy

A chemical reaction requires an energy barrier known as activation energy.

A catalyst provides an alternative reaction pathway with a lower activation energy.

Reactants → Transition State → Products

The catalyst stabilizes the transition state or provides a sequence of elementary steps that requires less activation energy than the uncatalysed pathway.

Remember: A catalyst lowers the activation energy but does not change the overall energy difference between reactants and products.

15. Effect of Catalyst on Chemical Equilibrium

A catalyst does not change the position of equilibrium.

In a reversible reaction, the catalyst lowers the activation energy for both the forward and reverse reactions.

Reactants ⇌ Products

Therefore, equilibrium is reached more rapidly, but the equilibrium composition remains unchanged.

The equilibrium constant is not changed by the presence of a catalyst.

16. Promoters

A promoter is a substance that increases the activity or efficiency of a catalyst without itself necessarily acting as the principal catalyst.

Example

In the Haber process, iron is the main catalyst and substances such as potassium compounds and aluminium oxide can act as promoters in industrial catalyst formulations.

N2 + 3H2 ⇌ 2NH3

17. Catalyst Poisons

Catalyst poisons are substances that decrease the activity of a catalyst, often by strongly adsorbing onto active sites.

Poisoning is particularly important in heterogeneous catalysis because the poison may block active surface sites.

Example

Sulfur-containing compounds can poison several metal catalysts.

Catalyst poisoning is one of the major reasons why industrial feed materials often require purification before entering catalytic processes.

18. Surface Catalysis

In heterogeneous catalysis, the catalytic reaction commonly occurs on the surface of a solid catalyst.

Main Steps

  1. Diffusion of reactants toward the catalyst surface.
  2. Adsorption of reactants on active sites.
  3. Activation of adsorbed molecules.
  4. Reaction between adsorbed species.
  5. Desorption of products.
  6. Regeneration of active sites.

The availability of active surface sites is therefore important for catalytic efficiency.

19. Role of Adsorption in Heterogeneous Catalysis

Adsorption brings reactant molecules onto the catalyst surface and can weaken existing chemical bonds, making the molecules more reactive.

Two broad types of adsorption are commonly discussed:

19.1 Physical Adsorption

Physical adsorption, or physisorption, involves relatively weak intermolecular forces.

19.2 Chemical Adsorption

Chemical adsorption, or chemisorption, involves stronger interaction between the adsorbate and catalyst surface and is particularly important in many catalytic reactions.

20. Contact Theory of Catalysis

According to the contact theory, reactant molecules become adsorbed on the catalyst surface and are brought into close contact.

The adsorbed molecules become activated and react to form products. The products then leave the surface, making the active sites available for another catalytic cycle.

General Representation

Reactants ⇌ Adsorbed reactants → Adsorbed products ⇌ Products

21. Intermediate Compound Theory

According to the intermediate compound theory, a catalyst may react temporarily with one or more reactants to form an unstable intermediate.

The intermediate subsequently reacts with another reactant to form the products and regenerate the catalyst.

General Representation

A + C → AC
AC + B → AB + C

Here C represents the catalyst. It participates in the individual steps but is regenerated in the overall reaction.

22. Specificity of Catalysts

Catalysts are often selective or specific. A particular catalyst may strongly favor one reaction pathway over competing pathways.

This property is particularly important in organic synthesis and industrial chemistry because it can improve product yield and reduce unwanted by-products.

23. Important Industrial Catalytic Processes

23.1 Haber Process

Ammonia is manufactured by catalytic reaction of nitrogen and hydrogen.

N2 + 3H2 ⇌ 2NH3

Finely divided iron-based catalysts are used in industrial practice.

23.2 Contact Process

Sulfur dioxide is oxidized to sulfur trioxide using a catalyst.

2SO2 + O2 ⇌ 2SO3

Vanadium(V) oxide is widely used as the catalyst in the industrial Contact process.

23.3 Hydrogenation

Nickel, palladium or platinum can catalyze hydrogenation reactions.

C=C + H2 Ni/Pt/Pd C-C

23.4 Ostwald Process

Ammonia is oxidized catalytically to nitric oxide in the industrial production of nitric acid.

4NH3 + 5O2 Pt-Rh 4NO + 6H2O

24. Catalytic Converters

Catalytic converters are used in automobile exhaust systems to reduce harmful gaseous pollutants.

Precious-metal catalysts such as platinum, palladium and rhodium may be used in catalytic converter systems.

Carbon Monoxide Oxidation

2CO + O2 → 2CO2

Hydrocarbon Oxidation

Hydrocarbon + O2 → CO2 + H2O

Catalytic converters therefore help reduce emissions of carbon monoxide, unburned hydrocarbons and nitrogen oxides.

25. Factors Affecting Catalytic Activity

25.1 Temperature

Temperature influences both the reaction rate and the adsorption of reactants on a catalyst surface. An optimum temperature is often required for maximum catalytic efficiency.

25.2 Surface Area

For many solid catalysts, increased surface area provides more active sites and can increase catalytic activity.

25.3 Catalyst Concentration

In homogeneous systems, increasing catalyst concentration can increase the reaction rate when catalyst concentration is a controlling factor.

25.4 Promoters

Promoters may enhance catalyst activity or stability.

25.5 Catalyst Poisons

Poisons reduce catalytic activity by blocking active sites or otherwise interfering with the catalytic mechanism.

25.6 Reactant Concentration

The concentration or partial pressure of reactants can influence the rate of catalytic reactions.

26. Catalytic Activity and Selectivity

Catalytic activity refers to the ability of a catalyst to increase the rate of a reaction.

Selectivity refers to the ability of a catalyst to favor formation of a desired product over competing products.

An industrial catalyst should ideally have high activity, high selectivity, adequate stability and sufficient resistance to poisoning.

27. Catalyst Supports

A catalyst support is a material on which an active catalytic substance is dispersed.

Supports can increase surface area, improve dispersion of the active component and enhance mechanical stability.

Common support materials include alumina, silica and activated carbon.

28. Importance of Catalysis in Biological Systems

Almost every living cell depends on enzyme-catalyzed reactions. Without enzymes, many biochemical reactions would proceed too slowly to support life.

Examples include:

29. Industrial Importance of Catalysis

Catalysis is one of the most important principles used in modern chemical industries.

30. Advantages of Catalysis

31. Important Types of Catalysis

Type Meaning Example
Positive catalysis Increases reaction rate. MnO₂ in H₂O₂ decomposition.
Negative catalysis Decreases reaction rate. Inhibitors in oxidation reactions.
Homogeneous catalysis Catalyst and reactants are in the same phase. Soluble acid/base catalysis.
Heterogeneous catalysis Catalyst and reactants are in different phases. Fe in Haber process.
Autocatalysis One product accelerates the reaction. Mn²⁺ in permanganate-oxalate reaction.
Enzyme catalysis Biological molecules catalyze biochemical reactions. Catalase decomposition of H₂O₂.

32. Important Catalytic Reactions for Revision

2H2O2 MnO₂ 2H2O + O2
N2 + 3H2 Fe 2NH3
2SO2 + O2 V₂O₅ 2SO3
4NH3 + 5O2 Pt-Rh 4NO + 6H2O
2CO + O2 catalyst 2CO2

33. Important Points for Examination

34. Chapter Summary

Catalysis is the phenomenon in which the rate of a chemical reaction is changed by the presence of a catalyst. Catalysts generally increase reaction rate by providing an alternative pathway with lower activation energy.

Catalysis may be homogeneous or heterogeneous. Other important forms include positive catalysis, negative catalysis, autocatalysis and enzyme catalysis.

In heterogeneous catalysis, adsorption of reactants on the catalyst surface is particularly important. The major steps include adsorption, activation, surface reaction and desorption.

Promoters can improve catalyst performance, whereas catalyst poisons reduce activity. Enzymes are highly specific biological catalysts that operate under relatively mild conditions.

Catalysis has enormous industrial importance in ammonia production, sulfuric acid production, nitric acid production, hydrogenation, petroleum processing and automobile emission control.

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